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Advanced LC–MS-based methods to study the co-occurrence and metabolization of multiple mycotoxins in cereals and cereal-based food

Authors: Alexandra , Stranska , Václavíková , Christopher Elliott, Black , Meneely , Hajšlová , Ezekiel Chibundu , Schuhmacher , Rudolf Krska

Publication Type: Journal article

Journal: Analytical And Bioanalytical Chemistry

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Abstract

Liquid chromatography (LC) coupled with mass spectrometry (MS) is widely used for the determination of mycotoxins in cereals and cereal-based products. In addition to the regulated mycotoxins, for which official control is required, LC–MS is often used for the screening of a large range of mycotoxins and/or for the identification and characterization of novel metabolites. This review provides insight into the LC–MS methods used for the determination of co-occurring mycotoxins with special emphasis on multiple-analyte applications. The first part of the review is focused on targeted LC–MS approaches using cleanup methods such as solid-phase extraction and immunoaffinity chromatography, as well as on methods based on minimum cleanup (quick, easy, cheap, effective, rugged, and safe; QuEChERS) and dilute and shoot. The second part of the review deals with the untargeted determination of mycotoxins by LC coupled with high-resolution MS, which includes also metabolomics techniques to study the fate of mycotoxins in plants.

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Alexandra,M. Stranska,M. Václavíková,M. Christopher,T.E Black,C. Meneely,J. Hajšlová,J. Ezekiel,C. Schuhmacher,R. Rudolf,K. . (2018). Advanced LC–MS-based methods to study the co-occurrence and metabolization of multiple mycotoxins in cereals and cereal-based food, 410 (), 801-801.

Alexandra,M. Stranska,M. Václavíková,M. Christopher,T.E Black,C. Meneely,J. Hajšlová,J. Ezekiel,C. Schuhmacher,R. Rudolf,K. . "Advanced LC–MS-based methods to study the co-occurrence and metabolization of multiple mycotoxins in cereals and cereal-based food" 410, no (), (2018): 801-801.

Alexandra,M. and Stranska,M. and Václavíková,M. and Christopher,T.E and Black,C. and Meneely,J. and Hajšlová,J. and Ezekiel,C. and Schuhmacher,R. and Rudolf,K. and . (2018). Advanced LC–MS-based methods to study the co-occurrence and metabolization of multiple mycotoxins in cereals and cereal-based food, 410 (), pp801-801.

AlexandraM, StranskaM, VáclavíkováM, ChristopherTE, BlackC, MeneelyJ, HajšlováJ, EzekielC, SchuhmacherR, RudolfK, . Advanced LC–MS-based methods to study the co-occurrence and metabolization of multiple mycotoxins in cereals and cereal-based food. 2018, 410 ():801-801.

Alexandra,Malachova , Stranska,M , Václavíková,M , Christopher,T Elliott, Black,C , Meneely,J , Hajšlová,Jana , Ezekiel,Chibundu , Schuhmacher,Rainer , and Rudolf,Krska . "Advanced LC–MS-based methods to study the co-occurrence and metabolization of multiple mycotoxins in cereals and cereal-based food", 410 . (2018) : 801-801.

A.Malachova S.M V.M C.T Elliott B.C M.J H.Jana E.Chibundu S.Rainer & R.Krska , "Advanced LC–MS-based methods to study the co-occurrence and metabolization of multiple mycotoxins in cereals and cereal-based food" vol.410, no., pp. 801-801, 2018.

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